High-pressure X-ray Diffraction Study of Diaspore

Crystal structure of a new high-pressure polymorph of topaz-OH

A new high-pressure form of topaz-OH (denoted here topaz-OH II) was obtained at 14 GPa and 1400 °C. The X-ray diffraction pattern of this phase can be indexed by an orthorhombic cell with a = 4.72318(5), b = 8.91480(9), and c = 2.77276(3) Å. The lengths of a and b are similar, but c is approximately a third of that for a previously reported topaz-OH (denoted topaz-OH I). The structural formula ...

X-ray Charge-Dens Study of 5-Chloro-8-hydroxy-6-methyloaphthalene-l.4-dione: A Hydroxynaphthoquinone Derivative

The X-ray charge density analysis of a hydroxynaphthoquinnne derivative was obtained by multipolar Hansen-Coppens formalism refinement through high resolution X-ray diffraction data at 100(1) K. The molecularproperties of the title compound resulted from the combined experimental and the quantum theory of atoms inmolecules (QTAIM) studies. The topological properties of the covalent bonds and of...

Introducing an Optimized Method for Obtaining X-ray Diffraction Patterns of Biological Tissues

Introduction Individual X-Ray diffraction patterns of biological tissues are obtained via interference of coherent scattering with their electrons. Many scientists have distinguished normal and cancerous breast tissue, bone density, and urinary stone types using the X-Ray diffraction patterns resulting from coherent scattering. The goal of this study was to introduce an optimized method for obt...

High pressure x-ray diffraction study of the volume collapse in Ba24Si100 clathrate

Amorphous boron gasket in diamond anvil cell research

Recent advances in high-pressure diamond anvil cell experiments include high-energy synchrotron x-ray techniques as well as new cell designs and gasketing procedures. The success of high-pressure experiments usually depends on a well-prepared sample, in which the gasket plays an important role. Various gasket materials such as diamond, beryllium, rhenium, and stainless steel have been used. Her...